Characterization (materials science)

{{Short description|Study of material structure and properties}}

File:Glockenbronze.jpg showing the micron scale dendritic microstructure of a bronze alloy]]

Characterization, when used in materials science, refers to the broad and general process by which a material's structure and properties are probed and measured. It is a fundamental process in the field of materials science, without which no scientific understanding of engineering materials could be ascertained.{{cite book|last1=Kumar|first1=Sam Zhang, Lin Li, Ashok|title=Materials characterization techniques|date=2009|publisher=CRC Press|location=Boca Raton|isbn=978-1420042948}} The scope of the term often differs; some definitions limit the term's use to techniques which study the microscopic structure and properties of materials,{{cite book |last= Leng|first= Yang|date= 2009|title= Materials Characterization: Introduction to Microscopic and Spectroscopic Methods|publisher= Wiley |isbn= 978-0-470-82299-9}} while others use the term to refer to any materials analysis process including macroscopic techniques such as mechanical testing, thermal analysis and density calculation.{{cite book |last= Zhang|first= Sam|date= 2008|title= Materials Characterization Techniques|publisher= CRC Press|isbn= 978-1420042948}} The scale of the structures observed in materials characterization ranges from angstroms, such as in the imaging of individual atoms and chemical bonds, up to centimeters, such as in the imaging of coarse grain structures in metals.

While many characterization techniques have been practiced for centuries, such as basic optical microscopy, new techniques and methodologies are constantly emerging. In particular the advent of the electron microscope and secondary ion mass spectrometry in the 20th century has revolutionized the field, allowing the imaging and analysis of structures and compositions on much smaller scales than was previously possible, leading to a huge increase in the level of understanding as to why different materials show different properties and behaviors.Mathys, Daniel, Zentrum für Mikroskopie, University of Basel: Die Entwicklung der Elektronenmikroskopie vom Bild über die Analyse zum Nanolabor, p. 8 More recently, atomic force microscopy has further increased the maximum possible resolution for analysis of certain samples in the last 30 years.[https://patents.google.com/patent/US4724318?oq=4724318 Patent US4724318 – Atomic force microscope and method for imaging surfaces with atomic resolution – Google Patents]

Microscopy

File:Aluminium Microstructure.jpg

File:Graphite ambient STM.jpg

Microscopy is a category of characterization techniques which probe and map the surface and sub-surface structure of a material. These techniques can use photons, electrons, ions or physical cantilever probes to gather data about a sample's structure on a range of length scales. Some common examples of microscopy techniques include:

Spectroscopy

Spectroscopy is a category of characterization techniques which use a range of principles to reveal the chemical composition, composition variation, crystal structure and photoelectric properties of materials. Some common examples of spectroscopy techniques include:

=Optical radiation=

=X-ray=

File:PIA16217-MarsCuriosityRover-1stXRayView-20121017.jpg analysis reveals feldspar, pyroxenes, olivine and more (Curiosity rover at "Rocknest", October 17, 2012).{{cite web |last=Brown |first=Dwayne |title=NASA Rover's First Soil Studies Help Fingerprint Martian Minerals |url=http://www.nasa.gov/home/hqnews/2012/oct/HQ_12-383_Curiosity_CheMin.html |date=October 30, 2012 |publisher=NASA |access-date=October 31, 2012}}]]

File:XRD+Rietveld-Fit-Y2Cu2O5.png with two phases, showing 1% of yttrium oxide impurity (red tickers)|400x400px]]

=Mass spectrometry=

{{further|Mass spectrometry}}

=Nuclear spectroscopy=

=Other=

Macroscopic testing

A huge range of techniques are used to characterize various macroscopic properties of materials, including:

File:(a) effective refractive indexes and (b) absorption coefficients of the electronic chips.jpg

See also

References

{{Reflist}}

{{Branches of chemistry}}

{{Branches of materials science}}

{{BranchesofSpectroscopy}}

{{Mass spectrometry}}

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Category:Materials science