Indium(III) nitrate

{{Chembox

|Section1={{Chembox Identifiers

| index_label=anhydrous

| index1_label=monohydrate

| index3_label=trihydrate

| index4_label=tetrahydrate

| index5_label=pentahydrate

| CASNo_Ref = {{cascite|correct|CAS}}

| CASNo = 13770-61-1

| CASNo1=13465-14-0

| CASNo3=15650-88-1

| ChemSpiderID = 24472

| ChemSpiderID1 = 2341257

| ChemSpiderID3 = 26948018

| PubChem=26265

| PubChem1=3084148

| PubChem3=91886655

| PubChem4=138753438

| PubChem5=22446589

| EC_number = 237-393-5

| RTECS = NL1750000

| UNII_Ref = {{fdacite|correct|FDA}}

| UNII = WOP84073FA

| SMILES = [N+](=O)([O-])[O-].[N+](=O)([O-])[O-].[N+](=O)([O-])[O-].[In+3]

| SMILES1 = [N+](=O)([O-])O[In](O[N+](=O)[O-])O[N+](=O)[O-].O

| SMILES3 = [N+](=O)([O-])O[In](O[N+](=O)[O-])O[N+](=O)[O-].O.O.O

| SMILES4 = [N+](=O)([O-])O[In](O[N+](=O)[O-])O[N+](=O)[O-].O.O.O.O

| StdInChI=1S/In.3NO3/c;3*2-1(3)4/q+3;3*-1

| StdInChIKey = LKRFCKCBYVZXTC-UHFFFAOYSA-N

| InChI1=1S/In.3NO3.H2O/c;3*2-1(3)4;/h;;;;1H2/q+3;3*-1;

| InChIKey1 = YZZFBYAKINKKFM-UHFFFAOYSA-N

| InChI3=1S/In.3NO3.3H2O/c;3*2-1(3)4;;;/h;;;;3*1H2/q+3;3*-1;;;

| InChIKey3 = HVDZMISZAKTZFP-UHFFFAOYSA-N

| InChI4=1S/In.3NO3.4H2O/c;3*2-1(3)4;;;;/h;;;;4*1H2/q+3;3*-1;;;;

| InChIKey4 = ZYYDOSLSINDXIQ-UHFFFAOYSA-N

}}

| Section2 = {{Chembox Properties

| AtmosphericOHRateConstant =

| Appearance = White solid

| BoilingPt =

| BoilingPtC =

| BoilingPt_ref =

| BoilingPt_notes=

| Density = 2.43 g/cm3 (pentahydrate)

| Formula = In(NO3)3

| HenryConstant =

| LogP =

| MolarMass = 300.83 g/mol

| MeltingPt =

| MeltingPtC = 100

| MeltingPt_ref =

| MeltingPt_notes= (decomposes, hydrate)

| pKa =

| pKb =

| Solubility = Soluble

| SolubleOther =

| Solvent =

| VaporPressure =

}}

| Section3 = {{Chembox Structure

| Structure_ref = {{cite journal |author1=M. A. Malyarik |author2=S. P. Petrosyants |author3=A. B. Ilyukhin |author4=Yu. A. Buslaev |title=Polyfunctionality of the nitrate group, coordination numbers of trivalent indium in nitrates complexes, and crystal structures of [In(NO3)(H2O)5](NO3)2 and HK6[In(NO3)4(H2O)2]3(NO3)4|journal=Russian Journal of Inorganic Chemistry |date=1993 |volume=38 |issue=12 |pages=1849–1854 |url=https://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=3854200 |issn=0036-0236}}

| CrystalStruct = Monoclinic

| SpaceGroup = C2/c

| LattConst_a = 10.35 Å

| LattConst_b = 9.17 Å

| LattConst_c = 11.25 Å

| LattConst_alpha =

| LattConst_beta = 91.05

| LattConst_gamma =

| LattConst_ref =

| LattConst_Comment =

| UnitCellVolume = 1068 Å3

| UnitCellFormulas =

| Coordination =

| MolShape =

| OrbitalHybridisation =

| Dipole =

}}

|Section7={{Chembox Hazards

| GHSPictograms = {{GHS03}}{{GHS07}}

| GHSSignalWord = Warning

| HPhrases = {{H-phrases|272|315|319|335}}

| PPhrases = {{P-phrases|210|220|221|261|264|271|280|302+352|304+340|305+351+338|312|321|332+313|337+313|362|370+378|403+233|405|501}}

}}

}}

Indium(III) nitrate is a nitrate salt of indium which forms various hydrates. Only the pentahydrate has been crystallographically verified. Other hydrates are also reported in literature, such as the trihydrate.{{cite journal |author1=Galina V. Kozhevnikova |author2=Gábor Keresztury |title=The state of indium ions in nitrate solutions: A Raman spectroscopic study |journal=Inorganica Chimica Acta |date=1985 |volume=98 |issue=1 |pages=59–65 |doi=10.1016/S0020-1693(00)90751-5 |language=en}}

Production and reactions

Indium(III) nitrate hydrate is produced by the dissolution of indium metal in concentrated nitric acid followed by evaporation of the solution:{{cite journal |author1=D. G. Tuck |author2=E. J. Woodhouse |author3=P. Carty |title=Co-ordination compounds of indium. Part III. Indium(III) nitrate species |journal=Journal of the Chemical Society A: Inorganic, Physical, Theoretical |date=1966 |pages=1077–1080 |doi=10.1039/J19660001077 |language=en}}

:{{chem2 | In + 4 HNO3 -> In(NO3)3 + NO + 2 H2O }}

The hydrate first decomposes to a basic salt and then to indium(III) oxide at 240 °C. Anhydrous indium(III) nitrate is claimed to be produced by the reaction of anhydrous indium(III) chloride and dinitrogen pentoxide.{{cite journal |author1=B. O. Field |author2=C. J. Hardy |title=Volatile and anhydrous nitrato-complexes of metals: preparation by the use of dinitrogen pentroxide, and measurement of infrared spectra |journal=Journal of the Chemical Society |date=1964 |pages=4428–4434 |doi=10.1039/JR9640004428 |language=en}}

In the presence of excess nitrate ions, indium(III) nitrate converts to the [In(NO3)4] ion.

The hydrolysis of indium(III) nitrate yields indium(III) hydroxide. It also reacts with sodium tungstate to form In(OH)WO4, [In(OH)2]2WO4, NaInWO4 or In2(WO4)3 depending on pH.{{cite journal |author1=Keita Yura |author2=Karl C. Fredrikson |author3=Egon Matijević |title=Preparation and properties of uniform colloidal indium compounds of different morphologies |journal=Colloids and Surfaces |date=1990 |volume=50 |pages=281–293 |doi=10.1016/0166-6622(90)80270-E |language=en}}{{cite journal | author = Shcherbina, K. G.; Mokhosoev, M. V.; Gruba, A. I. | title = Reaction of aluminum and indium nitrates with sodium tungstate in hot solutions | language = ru | journal = Zhurnal Neorganicheskoi Khimii | date = 1974 | volume = 19 | issue = 2 | pages = 396–399 | issn = 0044-457X }}

Structure

Only the pentahydrate has been structurally elucidated. The pentahydrate consists of octahedral [In(NO3)(H2O)5]2+ centers as well as two nitrates and is monoclinic.

References

{{Reflist}}

{{nitrates}}

{{Indium compounds}}

Category:Indium compounds

Category:Nitrates